C₄₉H₆₇BO₈

Base Information

Chemical Name:C₄₉H₆₇BO₈
CAS No.:392692-58-9
Molecular Formula:C₄₉H₆₇BO₈
Molecular Weight:794.877
Hs Code.:

C<sub>49</sub>H<sub>67</sub>BO<sub>8</sub>

Synonyms:C₄₉H₆₇BO₈

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Chemical Property of C₄₉H₆₇BO₈

Chemical Property:

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Technology Process of C₄₉H₆₇BO₈

There total 16 articles about C₄₉H₆₇BO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 194934-58-2
(S)-2-[5-(R)-benzyloxy-2,2,6-(6R)-trimethyl-1,3-dioxan-4-(R)-yl]-propionaldehyde

: 392692-58-9
C₄₉H₆₇BO₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: LiCl; i-Pr₂NEt / acetonitrile / 0.17 h / 20 °C

1.2: 96 percent / acetonitrile / 16 h / 20 °C

2.1: 98 percent / aq. AD-mix-β; MeSO2NH2 / 2-methyl-propan-2-ol / 16 h / 20 °C

3.1: 100 percent / NaHCO₃; H₂ / Pd(OH)2/C / methanol / 20 h / 20 °C

4.1: 97 percent / Ph₃CBF₄ / tetrahydrofuran / 0.5 h / 0 °C

5.1: 94 percent / DIBAL-H / CH₂Cl₂ / 1.5 h / -78 °C

6.1: Ba(OH)2*8H₂O / tetrahydrofuran / 0.5 h / 20 °C

6.2: 96 percent / tetrahydrofuran; H₂O / 4 h / 20 °C

7.1: aq. AcOH / tetrahydrofuran / 60 h / 20 °C

7.2: KOH / methanol / 20 h / 20 °C

8.1: 81 percent / toluene; tetrahydrofuran / 2 h / 120 °C

9.1: 94 percent / TPAP; 4 Angstroem molecular sieves; NMO / CH₂Cl₂ / 2 h / 20 °C

10.1: Et₃N / diethyl ether / 2.5 h / -78 °C

With barium dihydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; methanesulfonamide; 4 A molecular sieve; AD-mix-β; hydrogen; trityl tetrafluoroborate; diisobutylaluminium hydride; sodium hydrogencarbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; palladium dihydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; acetonitrile; tert-butyl alcohol; 1.2: Horner-Wadsworth-Emmons chain extension / 2.1: Sharpless asymmetric dihydroxylation / 6.2: Horner-Wadsworth-Emmons chain extension / 7.1: intramolecular hetero-Michael addition;
DOI:10.1039/b504149j

Reference yield:

: 862509-84-0
(4R,5R,6R)-5-benzyloxy-4-[1-hydroxy-prop-2-(R)-yl]-2,2,6-trimethyl-1,3-dioxane

: 392692-58-9
C₄₉H₆₇BO₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: 80 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

2.1: LiCl; i-Pr₂NEt / acetonitrile / 0.17 h / 20 °C

2.2: 96 percent / acetonitrile / 16 h / 20 °C

3.1: 98 percent / aq. AD-mix-β; MeSO2NH2 / 2-methyl-propan-2-ol / 16 h / 20 °C

4.1: 100 percent / NaHCO₃; H₂ / Pd(OH)2/C / methanol / 20 h / 20 °C

5.1: 97 percent / Ph₃CBF₄ / tetrahydrofuran / 0.5 h / 0 °C

6.1: 94 percent / DIBAL-H / CH₂Cl₂ / 1.5 h / -78 °C

7.1: Ba(OH)2*8H₂O / tetrahydrofuran / 0.5 h / 20 °C

7.2: 96 percent / tetrahydrofuran; H₂O / 4 h / 20 °C

8.1: aq. AcOH / tetrahydrofuran / 60 h / 20 °C

8.2: KOH / methanol / 20 h / 20 °C

9.1: 81 percent / toluene; tetrahydrofuran / 2 h / 120 °C

10.1: 94 percent / TPAP; 4 Angstroem molecular sieves; NMO / CH₂Cl₂ / 2 h / 20 °C

11.1: Et₃N / diethyl ether / 2.5 h / -78 °C

With barium dihydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; methanesulfonamide; 4 A molecular sieve; AD-mix-β; hydrogen; trityl tetrafluoroborate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; palladium dihydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; acetonitrile; tert-butyl alcohol; 2.2: Horner-Wadsworth-Emmons chain extension / 3.1: Sharpless asymmetric dihydroxylation / 7.2: Horner-Wadsworth-Emmons chain extension / 8.1: intramolecular hetero-Michael addition;
DOI:10.1039/b504149j

Reference yield:

: 194934-52-6
methyl (2E,4R)-4-[5-(R)-benzyloxy-2,2,6-(6R)-trimethyl-1,3-dioxan-4-(R)-yl]-pent-2-enoate

: 392692-58-9
C₄₉H₆₇BO₈

Guidance literature:: Multi-step reaction with 9 steps

1.1: 98 percent / aq. AD-mix-β; MeSO2NH2 / 2-methyl-propan-2-ol / 16 h / 20 °C

2.1: 100 percent / NaHCO₃; H₂ / Pd(OH)2/C / methanol / 20 h / 20 °C

3.1: 97 percent / Ph₃CBF₄ / tetrahydrofuran / 0.5 h / 0 °C

4.1: 94 percent / DIBAL-H / CH₂Cl₂ / 1.5 h / -78 °C

5.1: Ba(OH)2*8H₂O / tetrahydrofuran / 0.5 h / 20 °C

5.2: 96 percent / tetrahydrofuran; H₂O / 4 h / 20 °C

6.1: aq. AcOH / tetrahydrofuran / 60 h / 20 °C

6.2: KOH / methanol / 20 h / 20 °C

7.1: 81 percent / toluene; tetrahydrofuran / 2 h / 120 °C

8.1: 94 percent / TPAP; 4 Angstroem molecular sieves; NMO / CH₂Cl₂ / 2 h / 20 °C

9.1: Et₃N / diethyl ether / 2.5 h / -78 °C

With barium dihydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; methanesulfonamide; 4 A molecular sieve; AD-mix-β; hydrogen; trityl tetrafluoroborate; diisobutylaluminium hydride; sodium hydrogencarbonate; acetic acid; triethylamine; palladium dihydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; tert-butyl alcohol; 1.1: Sharpless asymmetric dihydroxylation / 5.2: Horner-Wadsworth-Emmons chain extension / 6.1: intramolecular hetero-Michael addition;
DOI:10.1039/b504149j