C₄₈H₆₈N₂O₈

Base Information

Chemical Name:C₄₈H₆₈N₂O₈
CAS No.:1313868-02-8
Molecular Formula:C₄₈H₆₈N₂O₈
Molecular Weight:801.077
Hs Code.:

C<sub>48</sub>H<sub>68</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₄₈H₆₈N₂O₈

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Chemical Property of C₄₈H₆₈N₂O₈

Chemical Property:

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Technology Process of C₄₈H₆₈N₂O₈

There total 6 articles about C₄₈H₆₈N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1313868-01-7
C₅₁H₇₆N₂O₈Si

: 1313868-02-8
C₄₈H₆₈N₂O₈

Guidance literature:: With potassium fluoride dihydrate; In chloroform; acetonitrile; at 40 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201003603

Reference yield:

: 1313867-96-7
C₂₄H₄₀N₂O₄

: 1313868-02-8
C₄₈H₆₈N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: iron(III) chloride; bromine / dichloromethane / Reflux

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

3: potassium carbonate / methanol; dichloromethane / 0.08 h / 20 °C / Inert atmosphere

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

5: potassium fluoride dihydrate / chloroform; acetonitrile / 1 h / 40 °C / Inert atmosphere

With iron(III) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium fluoride dihydrate; bromine; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetonitrile; 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1002/chem.201003603

Reference yield:

: 1313867-98-9
C₃₄H₅₆N₂O₄Si₂

: 1313868-02-8
C₄₈H₆₈N₂O₈

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol; dichloromethane / 0.08 h / 20 °C / Inert atmosphere

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

3: potassium fluoride dihydrate / chloroform; acetonitrile / 1 h / 40 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium fluoride dihydrate; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetonitrile; 2: Sonogashira coupling;
DOI:10.1002/chem.201003603