C₁₄H₁₃ClO₃S

Base Information

• Chemical Name: C₁₄H₁₃ClO₃S
• CAS No.: 1356488-11-3
• Molecular Formula: C₁₄H₁₃ClO₃S
• Molecular Weight: 296.774
• Mol file: 1356488-11-3.mol

Synonyms:C₁₄H₁₃ClO₃S

Chemical Property of C₁₄H₁₃ClO₃S

Chemical Property:

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Technology Process of C₁₄H₁₃ClO₃S

There total 1 articles about C₁₄H₁₃ClO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-acetyl-3-chlorothiophene (89581-82-8) + 2-6-dimethoxybenzoic acid (1466-76-8) → C14H13ClO3S (1356488-11-3)

Guidance literature:

With palladium diacetate; silver carbonate; tricyclohexylphosphine; In 1,2-dimethoxyethane; dimethyl sulfoxide; at 120 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.201106451

upstream raw materials:

2-acetyl-3-chlorothiophene

2-6-dimethoxybenzoic acid

Refernces