[2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester

Base Information

Chemical Name:[2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester
CAS No.:143209-69-2
Molecular Formula:C₂₆H₃₀N₂O₃
Molecular Weight:418.536
Hs Code.:

Synonyms:[2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester

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Chemical Property of [2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester

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Technology Process of [2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester

There total 3 articles about [2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 502-49-8
cycloactanone

: 143209-54-5
C₃₆H₃₁N₂O₃P

: 143209-69-2
[2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester

Guidance literature:: With 4 A molecular sieve; at 120 ℃; for 18h;
DOI:10.1016/S0040-4020(01)89032-3

Reference yield:

: 140701-23-1
3-Benzyl-3-bromo-2-oxo-2,3-dihydro-indole-1-carboxylic acid ethyl ester

: 143209-69-2
[2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / aq.NaN₃, tetrahexylammonium iodide / CH₂Cl₂ / 18 h / Ambient temperature

2: 70 percent / diethyl ether / 3 h / Ambient temperature

3: 50 percent / molecular sieves 4 Angstroem / 18 h / 120 °C

With sodium azide; 4 A molecular sieve; tetrahexylammonium iodide; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)89032-3

Reference yield:

: 143209-47-6
3-Azido-3-benzyl-2-oxo-2,3-dihydro-indole-1-carboxylic acid ethyl ester

: 143209-69-2
[2-(2-Benzyl-3-oxo-2,3,4,5,6,7,8,9-octahydro-1H-cycloocta[b]pyrrol-2-yl)-phenyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / diethyl ether / 3 h / Ambient temperature

2: 50 percent / molecular sieves 4 Angstroem / 18 h / 120 °C

With 4 A molecular sieve; In diethyl ether;
DOI:10.1016/S0040-4020(01)89032-3