9-hydroxy-β-damascone

Base Information

Chemical Name:9-hydroxy-β-damascone
CAS No.:80253-72-1
Molecular Formula:C₁₃H₂₀O₂
Molecular Weight:208.301
Hs Code.:

Synonyms:9-hydroxy-β-damascone

Suppliers and Price of 9-hydroxy-β-damascone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-hydroxy-β-damascone

Chemical Property:

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Technology Process of 9-hydroxy-β-damascone

There total 1 articles about 9-hydroxy-β-damascone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 77250-07-8
3-diazo-4-hydroxy-4-(2,6,6-trimethylcyclohex-1-enyl)butan-2-one

: 80253-72-1
9-hydroxy-β-damascone

Guidance literature:: rhodium(II) acetate; In 1,2-dimethoxyethane; at 45 ℃; for 3h;
DOI:10.1039/P19810002566

Reference yield: 16.6%

: 80253-72-1
9-hydroxy-β-damascone

: 77250-09-0
(Z)-3-chloro-1-(2,6,6-trimethylcyclohex-1-enyl)but-2-en-1-one

: 77250-10-3
(E)-3-chloro-1-(2,6,6-trimethylcyclohex-1-enyl)but-2-en-1-one

Guidance literature:: With oxalyl dichloride; In chloroform; for 3h; Heating;
DOI:10.1039/P19810002566

Reference yield:

: 80253-72-1
9-hydroxy-β-damascone

: 23726-91-2
beta damascone

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / oxalyl chloride / CHCl₃ / 3 h / Heating

2: 60 percent / silver-zinc couple / methanol / 21 h / Ambient temperature

With oxalyl dichloride; zinc silver; In methanol; chloroform;
DOI:10.1039/P19810002566