(S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine

Base Information

• Chemical Name: (S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine
• CAS No.: 862121-83-3
• Molecular Formula: C₂₄H₂₉NO₃
• Molecular Weight: 379.499

Synonyms:(S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine

Chemical Property of (S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine

Chemical Property:

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Technology Process of (S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine

There total 1 articles about (S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(Z,E)-1,3-hexadien-1-amine (862121-74-2) → (S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine (862121-83-3)

Guidance literature:

With trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; for 1.5h;

DOI:10.1021/jo047752m

Reference yield: 80.3%

cyclopent-1-enylmethyl-(4-methoxyphenyl)-carbamic acid tert-butyl ester (862121-73-1) + (S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine (862121-83-3) → {2-[(4-bromophenyl)-hydroxy-methyl]-cyclopentylidenemethyl}-(4-methoxyphenyl)-carbamic acid tert-butyl ester + {2-[(4-bromophenyl)-hydroxy-methyl]-cyclopentylidenemethyl}-(4-methoxyphenyl)-carbamic acid tert-butyl ester

Guidance literature:

cyclopent-1-enylmethyl-(4-methoxyphenyl)-carbamic acid tert-butyl ester; With n-butyllithium; (-)-sparteine; In toluene; at -78 ℃; for 2h;

(S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine; In toluene; at -78 ℃; for 2h;

DOI:10.1021/jo047752m

Reference yield: 79.0%

(S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(E,E)-1,3-hexadien-1-amine (862121-83-3) + N-methylmaleimide (930-88-1) → (4-methoxyphenyl)-[2-methyl-1,3-dioxo-7-(1-phenylethyl)-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl]-carbamic acid tert-butyl ester

Guidance literature:

In toluene; for 12h; Heating;

DOI:10.1021/jo047752m

upstream raw materials:

(S)-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-5-phenyl-(Z,E)-1,3-hexadien-1-amine

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