7-chloro-5-(2-chlorophenyl)-1,3-dihydro-2H-thieno-(2,3-e)-(1,4)-diazepine-2-thione

Base Information

• Chemical Name: 7-chloro-5-(2-chlorophenyl)-1,3-dihydro-2H-thieno-(2,3-e)-(1,4)-diazepine-2-thione
• CAS No.: 54123-07-8
• Molecular Formula: C13H8 Cl2 N2 S2
• Molecular Weight: 327.25
• Hs Code.: 2934999090
• Mol file: 54123-07-8.mol

Synonyms:7-chloro-5-(2-chlorophenyl)-1,3-dihydro-2H-thieno-(2,3-e)-(1,4)-diazepine-2-thione

Chemical Property of 7-chloro-5-(2-chlorophenyl)-1,3-dihydro-2H-thieno-(2,3-e)-(1,4)-diazepine-2-thione

Chemical Property:

• Vapor Pressure: 1.91E-10mmHg at 25°C
• Boiling Point: 508.1°Cat760mmHg
• Flash Point: 261.1°C
• PSA: 84.72000
• Density: 1.57g/cm³
• LogP: 2.52600

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-chloro-5-(2-chlorophenyl)-1,3-dihydro-2H-thieno-(2,3-e)-(1,4)-diazepine-2-thione

There total 1 articles about 7-chloro-5-(2-chlorophenyl)-1,3-dihydro-2H-thieno-(2,3-e)-(1,4)-diazepine-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 7-chloro-5-(2-chloro-phenyl)-1,3-dihydro-thieno[2,3-e][1,4]diazepine-2-thione (54123-07-8)

Guidance literature:

Entspr. 2-Keto-Verb., P4S10;

Reference yield:

7-chloro-5-(2-chloro-phenyl)-1,3-dihydro-thieno[2,3-e][1,4]diazepine-2-thione (54123-07-8) + 7-chloro-5-(2-chloro-phenyl)-1,3-dihydro-thieno[2,3-e][1,4]diazepin-2-one (36811-59-3) + butan-1-ol (71-36-3) → 2-(2-acetylhydrazino)-7-chloro-5-(o-chlorophenyl)-3H-thieno[2,3-e]-1,4-diazepine

Guidance literature:

With diphosphorus pentasulfide; In pyridine; ethanol; water; ethyl acetate;

Reference yield:

7-chloro-5-(2-chloro-phenyl)-1,3-dihydro-thieno[2,3-e][1,4]diazepine-2-thione (54123-07-8) → 7-chloro-5-(o-chlorophenyl)-2-(2-lactoylhydrazino)-3H-thieno[2,3-e]-1,4-diazepine

Guidance literature:

In methanol;

Downstream raw materials:

2-chloro-4-(o-chlorophenyl)-9-[(p-methoxybenzyloxy)methyl]-6H-thieno[3,2-f]-s-triazolo[4,3-a][1,4]diazepine

2-chloro-4-(o-chlorophenyl)-6H-thieno[3,2-f]-s-triazolo[4,3-a][1,4]-diazepine-9-carboxylic acid ethyl ester

2-chloro-4-(2-chloro-phenyl)-6H-[1,2,4]triazolo[4,3-a]thieno[3,2-f][1,4]diazepine-9-carboxylic acid amide

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