N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide

Base Information

• Chemical Name: N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide
• CAS No.: 1137520-59-2
• Molecular Formula: C₁₈H₂₀N₂O₅S₂
• Molecular Weight: 408.499

Synonyms:N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide

Chemical Property of N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide

Chemical Property:

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Technology Process of N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide

There total 1 articles about N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-[(Z)-4-bromobut-2-enyl]-N-(4-methoxy-2-nitrophenyl)methanesulfonamide (1137520-56-9) + thiophenol (108-98-5) → N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide (1137520-59-2)

Guidance literature:

thiophenol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 25 ℃; for 1h; Inert atmosphere;

N-[(Z)-4-bromobut-2-enyl]-N-(4-methoxy-2-nitrophenyl)methanesulfonamide; In tetrahydrofuran; mineral oil; at 0 - 25 ℃; for 5h; Inert atmosphere;

DOI:10.3762/bjoc.5.1

Reference yield: 91.0%

N-(4-methoxy-2-nitrophenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide (1137520-59-2) → N-(2-amino-4-methoxyphenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide (1137520-65-0)

Guidance literature:

With tin(ll) chloride; In methanol; dichloromethane; at 65 ℃; for 4h; Inert atmosphere;

DOI:10.3762/bjoc.5.1

upstream raw materials:

N-[(Z)-4-bromobut-2-enyl]-N-(4-methoxy-2-nitrophenyl)methanesulfonamide

thiophenol

Downstream raw materials:

N-(2-amino-4-methoxyphenyl)-N-[(Z)-4-phenylsulfanylbut-2-enyl]methanesulfonamide

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