5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol

Base Information

• Chemical Name: 5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol
• CAS No.: 793682-31-2
• Molecular Formula: C₃₂H₂₉N₃O
• Molecular Weight: 471.602

Synonyms:5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol

Chemical Property of 5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol

Chemical Property:

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Technology Process of 5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol

There total 3 articles about 5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-[1-(1-hydroxy-5-nitro-1,2,3,4-tetrahydronaphthyl)]-1-tritylimidazole (344765-75-9) → 5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol (793682-31-2)

Guidance literature:

With iron; ammonium chloride; In ethanol; Heating;

DOI:10.1021/jm030551a

Reference yield:

5-nitro-1-tetralone (51114-73-9) → 5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol (793682-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: EtMgBr / CH₂Cl₂; diethyl ether / 0.5 h

1.2: 63 percent / CH₂Cl₂; diethyl ether / 20 °C

2.1: 80 percent / aq. NH₄Cl; Fe / ethanol / Heating

With ethylmagnesium bromide; iron; ammonium chloride; In diethyl ether; ethanol; dichloromethane;

DOI:10.1021/jm030551a

Reference yield:

N-trityl-4(5)-iodoimidazole (96797-15-8) → 5-amino-1-(1-trityl-1H-imidazol-4-yl)-1,2,3,4-tetrahydro-naphthalen-1-ol (793682-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: EtMgBr / CH₂Cl₂; diethyl ether / 0.5 h

1.2: 63 percent / CH₂Cl₂; diethyl ether / 20 °C

2.1: 80 percent / aq. NH₄Cl; Fe / ethanol / Heating

With ethylmagnesium bromide; iron; ammonium chloride; In diethyl ether; ethanol; dichloromethane;

DOI:10.1021/jm030551a

upstream raw materials:

4-[1-(1-hydroxy-5-nitro-1,2,3,4-tetrahydronaphthyl)]-1-tritylimidazole

5-nitro-1-tetralone

N-trityl-4⁽⁵⁾-iodoimidazole

Downstream raw materials:

ethanesulfonic acid [5-hydroxy-5-(1-trityl-1H-imidazol-4-yl)-5,6,7,8-tetrahydro-naphthalen-1-yl]-amide

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