Technology Process of C13H9FO3S
There total 4 articles about C13H9FO3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; lithium hydroxide;
In
ethanol;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / N,N-dimethyl-formamide / 80 °C / 760.05 Torr
2: lithium hydroxide; water / ethanol / 20 °C
With
1,3-bis-(diphenylphosphino)propane; water; palladium diacetate; triethylamine; lithium hydroxide;
In
ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / dichloromethane / 0.17 h / Cooling with ice
1.2: 20 °C / Cooling with ice
2.1: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / N,N-dimethyl-formamide / 80 °C / 760.05 Torr
3.1: lithium hydroxide; water / ethanol / 20 °C
With
aluminum (III) chloride; 1,3-bis-(diphenylphosphino)propane; water; palladium diacetate; triethylamine; lithium hydroxide;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;