1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride

Base Information

Chemical Name:1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride
CAS No.:1431303-45-5
Molecular Formula:C₁₇H₁₄N₃O₄*Cl
Molecular Weight:359.769
Hs Code.:

Synonyms:1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride

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Chemical Property of 1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride

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Technology Process of 1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride

There total 4 articles about 1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1431303-50-2
1,4-bis(methyl 4-benzoate)-1-methyl-1H-1,2,3-triazolium triflate

: 1431303-45-5
1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride

Guidance literature:: 1,4-bis(methyl 4-benzoate)-1-methyl-1H-1,2,3-triazolium triflate; With potassium hydroxide; In methanol; for 16h; Reflux;

With hydrogenchloride; In methanol; water; at 20 ℃; pH=1 - 2;
DOI:10.1071/CH12462

Reference yield:

: 20442-96-0
methyl 4-azidobenzoate

: 1431303-45-5
1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / ethanol; water / 16 h / Inert atmosphere; Reflux

2.1: 1,1,2,2-tetrachloroethane / 16 h / 150 °C

3.1: potassium hydroxide / methanol / 16 h / Reflux

3.2: 20 °C / pH 1 - 2

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; potassium hydroxide; In methanol; ethanol; water; 1,1,2,2-tetrachloroethane;
DOI:10.1071/CH12462

Reference yield:

: 1431303-48-8
1,4-bis(methyl 4-benzoate)-1H-1,2,3-triazole

: 1431303-45-5
1,4-bis(4-benzoic acid)-1-methyl-1H-1,2,3-triazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1,2,2-tetrachloroethane / 16 h / 150 °C

2.1: potassium hydroxide / methanol / 16 h / Reflux

2.2: 20 °C / pH 1 - 2

With potassium hydroxide; In methanol; 1,1,2,2-tetrachloroethane;
DOI:10.1071/CH12462