C₄₇H₅₃N₇O₇

Base Information

Chemical Name:C₄₇H₅₃N₇O₇
CAS No.:1369595-45-8
Molecular Formula:C₄₇H₅₃N₇O₇
Molecular Weight:827.981
Hs Code.:

C<sub>47</sub>H<sub>53</sub>N<sub>7</sub>O<sub>7</sub>

Synonyms:C₄₇H₅₃N₇O₇

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Chemical Property of C₄₇H₅₃N₇O₇

Chemical Property:

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Technology Process of C₄₇H₅₃N₇O₇

There total 11 articles about C₄₇H₅₃N₇O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1007882-59-8
(S)-2-(4-bromo-1H-imidazol-2-yl)pyrrolidine-1-carboxylic acid tert-butyl ester

: 1369595-44-7
C₃₅H₄₁B₂NO₇

: 1369595-45-8
C₄₇H₅₃N₇O₇

Guidance literature:: With potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; at 90 ℃; for 17h;

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1369595-45-8
C₄₇H₅₃N₇O₇

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / ethanol / 6 h / Reflux

2: polyphosphoric acid / 2 h / 80 °C

3: caesium carbonate / dimethyl sulfoxide / 18 h / 90 °C

4: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 0.75 h / 90 °C / Inert atmosphere; Microwave irradiation

5: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 17 h / 90 °C

With potassium acetate; potassium carbonate; caesium carbonate; acetic acid; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 69610-40-8
N-(tert-butoxycarbonyl)-L-prolinol

: 1369595-45-8
C₄₇H₅₃N₇O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / Cooling with ice

2.1: ammonia / methanol / 0.5 h / 20 - 30 °C

2.2: 16 h / 20 - 60 °C

3.1: N-Bromosuccinimide / dichloromethane / 1.25 h / Cooling with ice

4.1: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 17 h / 90 °C

With N-Bromosuccinimide; oxalyl dichloride; ammonia; potassium carbonate; dimethyl sulfoxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; dichloromethane; water;