N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Base Information

Chemical Name:N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide
CAS No.:153093-16-4
Molecular Formula:C₂₉H₃₇NO₁₂
Molecular Weight:591.612
Hs Code.:

N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Synonyms:N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Suppliers and Price of N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

There total 6 articles about N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 153093-15-3
Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[(4aR,6R,7R,8R,8aS)-7-acetylamino-6-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-tetrahydro-pyran-3-yl ester

: 153093-16-4
N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: With triethylamine; In methanol; water; for 48h; Ambient temperature;
DOI:10.1039/c39930001419

Reference yield:

: 529493-92-3
2-(acetoxymethyl)-6-bromotetrahydro-2H-pyran-3,4,5-triyl triacetate

: 153093-16-4
N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Hg(CN)2, mol. sieve 4A / nitromethane; toluene

2: 93 percent / Et₃N / methanol; H₂O / 48 h / Ambient temperature

With 4 A molecular sieve; mercury(II) cyanide; triethylamine; In methanol; nitromethane; water; toluene;
DOI:10.1039/c39930001419

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 153093-16-4
N-[(4aR,6R,7R,8R,8aS)-6-(4-Methoxy-benzyloxy)-2-phenyl-8-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: TsOH / tetrahydrofuran

2: 100 percent / Hg(CN)2, mol. sieve 4A / nitromethane; toluene

3: 93 percent / Et₃N / methanol; H₂O / 48 h / Ambient temperature

With 4 A molecular sieve; mercury(II) cyanide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; nitromethane; water; toluene;
DOI:10.1039/c39930001419