(Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ⁵-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester

Base Information

• Chemical Name: (Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ⁵-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester
• CAS No.: 699023-60-4
• Molecular Formula: C₂₂H₃₁N₃O₄P₂
• Molecular Weight: 463.453

Synonyms:(Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ⁵-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester

Chemical Property of (Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ⁵-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ⁵-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester

There total 2 articles about (Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ⁵-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-(-)-(Z)-3-hexen-2-ol (148261-32-9) → (Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ5-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester (699023-60-4)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 6 h / 20 °C

2: benzene / 0.5 h

In benzene;

DOI:10.1002/anie.200353284

Reference yield:

diphenyl phosphoryl azide (26386-88-9) + 1,3-Dimethyl-2-((Z)-(S)-1-methyl-pent-2-enyloxy)-[1,3,2]diazaphospholidine → (Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ5-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester (699023-60-4)

Guidance literature:

In benzene; for 0.5h;

DOI:10.1002/anie.200353284

Reference yield:

(Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ5-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester (699023-60-4) → (E)-(R)-(1,3-dimethyl-2-oxo-2λ5-[1,3,2]diazaphospholidin-2-yl)-(1-ethyl-but-2-enyl)-phosphoramidic acid diphenyl ester (699023-75-1) + (E)-(S)-(1,3-dimethyl-2-oxo-2λ5-[1,3,2]diazaphospholidin-2-yl)-(1-ethyl-but-2-enyl)-phosphoramidic acid diphenyl ester

Guidance literature:

With dichloro bis(acetonitrile) palladium(II); 4 A molecular sieve; In dichloromethane; for 16h; Title compound not separated from byproducts;

DOI:10.1021/ja054161k

upstream raw materials:

diphenyl phosphoryl azide

(S)-(-)-(Z)-3-hexen-2-ol

Downstream raw materials:

(E)-(R)-(1,3-dimethyl-2-oxo-2λ⁵-[1,3,2]diazaphospholidin-2-yl)-(1-ethyl-but-2-enyl)-phosphoramidic acid diphenyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 699023-60-4 (Z)-(S)-[1,3-dimethyl-2-(1-methyl-pent-2-enyloxy)-2λ⁵-[1,3,2]diazaphospholidin-2-ylidene]-phosphoramidic acid diphenyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send