erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide

Base Information

Chemical Name:erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide
CAS No.:120713-24-8
Molecular Formula:C₁₇H₂₈ClN₃O₃
Molecular Weight:357.881
Hs Code.:

Synonyms:erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide

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Technology Process of erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide

There total 4 articles about erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 102670-59-7
butanopride hydrochloride

: 120713-24-8
erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 0.666667h; Heating;
DOI:10.1021/jm00403a011

Reference yield:

: 4-amino-2-(2-butanon-3-yl)oxy-5-chloro-N-[2-(diethylamino)ethyl]benzamide

: 102670-59-7
butanopride hydrochloride

: 120713-24-8
erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide

Guidance literature:: With sodium borohydrid; ammonia; In methanol; ethanol; dichloromethane;

Reference yield:

: 364-62-5
metoclopramide

: 120713-24-8
erythro-4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-hydroxybut-3-yl)oxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / sodium hydride, ethanethiol / dimethylformamide / 1.5 h / 100 - 105 °C

2: 81 percent / K₂CO₃, NaI / dimethylformamide / 16 h / Ambient temperature

3: 42 percent / NaBH₄ / ethanol / 0.67 h / Heating

With sodium tetrahydroborate; sodium hydride; potassium carbonate; ethanethiol; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00403a011