4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide

Base Information

• Chemical Name: 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide
• CAS No.: 459425-55-9
• Molecular Formula: C₃₂H₂₂N₄O₂
• Molecular Weight: 494.552
• Mol file: 459425-55-9.mol

Synonyms:4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide

Chemical Property of 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide

Chemical Property:

Purity/Quality:

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Technology Process of 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide

There total 1 articles about 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine (158982-94-6) → 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide (459425-55-9)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1039/b203087j

Reference yield: 85.0%

terbium(III) perchlorate + acetonitrile (75-05-8,26809-02-9) + 4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine-1,1'''-bisoxide (459425-55-9) → [Tb(4',4''-diphenyl-2,2':6',2'':6'',2''-quaterpyridine-1,1'''-O2)2][ClO4]3*2CH3CN

Guidance literature:

In ethanol; metal perchlorate salt was dissolved in min amount of ethanol and added to a suspn. of ligand in hot ethanol; ppt. was filtered, recrystd. by vapor diffusion of diethyl ether into a CH3CN soln.; elem. anal.;

DOI:10.1039/b203087j

upstream raw materials:

4',4''-diphenyl-2,2':6',2'':6'',2'''-quaterpyridine