Technology Process of C23H40FNO2Si
There total 5 articles about C23H40FNO2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanotrihydroborate; ammonium acetate;
In
methanol;
at 22 ℃;
for 48h;
DOI:10.1021/bc300266y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methyl vinyl ketone; sec.-butyllithium; copper(l) iodide / 1.5 h / -78 °C
2: sodium hydrogencarbonate / methanol / 25 °C
3: ammonium acetate; sodium cyanotrihydroborate / methanol / 48 h / 22 °C
With
copper(l) iodide; sodium cyanotrihydroborate; ammonium acetate; sec.-butyllithium; sodium hydrogencarbonate; methyl vinyl ketone;
In
methanol;
DOI:10.1021/bc300266y
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrahydrofuran / 1 h / 0 °C
2: sodium hydride / N,N-dimethyl-formamide / 15 h / 22 °C
3: methyl vinyl ketone; sec.-butyllithium; copper(l) iodide / 1.5 h / -78 °C
4: sodium hydrogencarbonate / methanol / 25 °C
5: ammonium acetate; sodium cyanotrihydroborate / methanol / 48 h / 22 °C
With
copper(l) iodide; sodium cyanotrihydroborate; ammonium acetate; sec.-butyllithium; sodium hydride; sodium hydrogencarbonate; methyl vinyl ketone;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
1: |Grignard Reaction / 2: |Williamson Ether Synthesis;
DOI:10.1021/bc300266y
