[1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane

Base Information

Chemical Name:[1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane
CAS No.:765300-59-2
Molecular Formula:C₄₈H₅₀O₃Si
Molecular Weight:703.009
Hs Code.:

[1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-<i>tert</i>-butyl-diphenyl-silane

Synonyms:[1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane

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Chemical Property of [1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane

Chemical Property:

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Technology Process of [1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane

There total 6 articles about [1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 765300-58-1
(3S,5R)-5-Benzyloxy-6-trityloxy-hex-1-en-3-ol

: 765300-59-2
[1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/j.tetasy.2004.06.023

Reference yield:

: 96852-88-9
3,5,6-trideoxy-1,2-O-isopropylidene-α-D-ribo-hex-5-enofuranoside

: 765300-59-2
[1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 6 steps

1: 79 percent / H₂SO₄ / 12 h / 60 °C

2: 75 percent / NaH / tetrahydrofuran / 6 h / 20 °C

3: 90 percent / H₂SO₄; aq. AcOH / 12 h / 60 °C

4: 90 percent / NaBH₄ / methanol / 1 h / 20 °C

5: 78 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

6: 70 percent / imidazole / CH₂Cl₂ / 4 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; sulfuric acid; sodium hydride; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetasy.2004.06.023

Reference yield:

: 258873-33-5
(3R,5S)-3-Benzyloxy-2-methoxy-5-vinyl-tetrahydro-furan

: 765300-59-2
[1-(2-benzyloxy-3-trityloxy-propyl)-allyloxy]-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / H₂SO₄; aq. AcOH / 12 h / 60 °C

2: 90 percent / NaBH₄ / methanol / 1 h / 20 °C

3: 78 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

4: 70 percent / imidazole / CH₂Cl₂ / 4 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; sulfuric acid; acetic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2004.06.023