6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

Base Information

Chemical Name:6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid
CAS No.:106139-07-5
Molecular Formula:C₂₂H₂₄BrN₃O₅
Molecular Weight:494.322
Hs Code.:

Synonyms:6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

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Chemical Property of 6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

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Technology Process of 6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

There total 1 articles about 6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1,6-Di-O-acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α,β-D-glucopyranose

: 106139-07-5
6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

Guidance literature:: With titanium(IV) bromide; In dichloromethane; ethyl acetate; for 12h;

Reference yield: 82.0%

: 106139-07-5
6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

: 100-51-6,185532-71-2
benzyl alcohol

: 106115-81-5
Benzyl-6-O-acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid

Guidance literature:: With silver silicate; 4 A molecular sieve; In dichloromethane; at -20 ℃; for 2h;

Reference yield:

: 106139-07-5
6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

: 106115-93-9
Benzyl-6-O-<6-O-acetyl-2-amino-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosyl>-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 2 h / -20 °C

2: 1 M NaOMe / CH₂Cl₂; methanol / 2 h

3: 70 percent / silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 4 h / -20 °C

4: 1.) H₂S, 2.) 0.5 N HCl / 1.) pyridine, H₂O, 6 h, 45 deg C, 2.) toluene, MeOH, 0 deg C

With hydrogenchloride; silver silicate; 4 A molecular sieve; hydrogen sulfide; sodium methylate; In methanol; dichloromethane;