4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide

Base Information

• Chemical Name: 4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide
• CAS No.: 86724-17-6
• Molecular Formula: C₁₉H₂₂N₂O₂S
• Molecular Weight: 342.462
• Mol file: 86724-17-6.mol

Synonyms:4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide

Chemical Property of 4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide

There total 1 articles about 4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-phenyl-4-cyclohexanone (4894-75-1) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide (86724-17-6)

Guidance literature:

In ethanol; at 100 ℃; for 1h;

DOI:10.1021/ja8016076

Reference yield: 94.0%

Z-α-bromostilbene (15022-93-2,40389-50-2) + 4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide (86724-17-6) → (E)-4-(1,2-diphenylvinyl)-1,2,3,6-tetrahydro-1,1'-biphenyl

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium tert-butoxide; XPhos; In 1,4-dioxane; at 130 ℃; for 12h; Inert atmosphere;

DOI:10.1002/adsc.201601155

Reference yield: 93.0%

4-methyl-N’-(4-phenylcyclohexylidene)benzenesulfono hydrazide (86724-17-6) + (E)-4-chlorostyrylboronic acid (154230-29-2) → 1-chloro-4-(2-(4-phenylcyclohexylidene)ethyl)benzene (1393683-18-5)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; methanol; at 150 ℃; for 0.5h; regioselective reaction; Microwave irradiation;

DOI:10.1002/anie.201200683

upstream raw materials:

1-phenyl-4-cyclohexanone

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

trans-N-(4-phenylcyclohexyl)-N'-tosylhydrazine

trans-N-(4-phenyl-1-deuterocyclohexyl)-N'-tosylhydrazine

1-phenyl-4-cyclohexanone

trans-4-phenylcyclohexan-1-d-1-ol