C₃₃H₄₀N₄O₆

Base Information

Chemical Name:C₃₃H₄₀N₄O₆
CAS No.:1428265-78-4
Molecular Formula:C₃₃H₄₀N₄O₆
Molecular Weight:588.704
Hs Code.:

C<sub>33</sub>H<sub>40</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:C₃₃H₄₀N₄O₆

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Chemical Property of C₃₃H₄₀N₄O₆

Chemical Property:

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Technology Process of C₃₃H₄₀N₄O₆

There total 13 articles about C₃₃H₄₀N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428265-74-0
C₃₃H₃₉N₄O₉S^(1-)*Na⁽¹⁺⁾

: 1428265-78-4
C₃₃H₄₀N₄O₆

Guidance literature:: With sulfuric acid; In tetrahydrofuran; water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.01.070

Reference yield:

: 14131-84-1
2,3:5,6-di-O-isopropylidene-α-D-mannofuranose

: 1428265-78-4
C₃₃H₄₀N₄O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: acetic acid / 3 h / Inert atmosphere; Reflux

3.1: thionyl chloride / tetrachloromethane / 0.5 h / Inert atmosphere; Reflux

3.2: 1 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: sulfuric acid / water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With thionyl chloride; sulfuric acid; sodium hydride; acetic acid; In tetrahydrofuran; tetrachloromethane; water;
DOI:10.1016/j.bmc.2013.01.070

Reference yield:

: 54469-08-8,74912-00-8,74912-01-9,20689-02-5
phenylmethyl 2,3:5,6-di-O-(1-methylethylidene)-α-D-mannofuranoside

: 1428265-78-4
C₃₃H₄₀N₄O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / 3 h / Inert atmosphere; Reflux

2.1: thionyl chloride / tetrachloromethane / 0.5 h / Inert atmosphere; Reflux

2.2: 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: sulfuric acid / water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With thionyl chloride; sulfuric acid; sodium hydride; acetic acid; In tetrahydrofuran; tetrachloromethane; water;
DOI:10.1016/j.bmc.2013.01.070