1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester

Base Information

Chemical Name:1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester
CAS No.:1311402-89-7
Molecular Formula:C₂₀H₂₇ClO₇
Molecular Weight:414.883
Hs Code.:

Synonyms:1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester

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Chemical Property of 1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester

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Technology Process of 1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester

There total 2 articles about 1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.5%

: 109-87-5
Dimethoxymethane

: 1311402-88-6
1-(4-chlorobenzyl)-3,3-bis(hydroxymethyl)-2-oxocyclopentane carboxylic acid methyl ester

: 1311402-89-7
1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester

Guidance literature:: Dimethoxymethane; 1-(4-chlorobenzyl)-3,3-bis(hydroxymethyl)-2-oxocyclopentane carboxylic acid methyl ester; With toluene-4-sulfonic acid; lithium bromide; In chloroform; at 20 ℃; for 2h;

With sodium hydrogencarbonate; In chloroform; water;

Reference yield:

: 115851-73-5
1-[(4-chlorophenyl)methyl]-2-oxocyclopentanecarboxylic acid methyl ester

: 1311402-89-7
1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; water / 5 h / 20 °C

2: toluene-4-sulfonic acid; lithium bromide / chloroform / 2 h / 20 °C

With potassium carbonate; toluene-4-sulfonic acid; lithium bromide; In tetrahydrofuran; chloroform; water;

Reference yield: 89.0%

: 1311402-89-7
1-(4-chlorobenzyl)-3,3-bis((methoxymethoxy)methyl)-2-oxocyclopentane carboxylic acid methyl ester

: 1311402-90-0
5-(4-chlorobenzyl)-2,2-bis((methoxymethoxy)methyl)cyclopentanone

Guidance literature:: With acetic acid; triethylamine; In N,N-dimethyl acetamide; at 155 - 165 ℃; for 23h; Reagent/catalyst; Solvent; Temperature; Time;