methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate

Base Information

• Chemical Name: methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate
• CAS No.: 1042152-17-9
• Molecular Formula: C₂₈H₃₉N₃O₄Si
• Molecular Weight: 509.721

Synonyms:methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate

Chemical Property of methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate

Chemical Property:

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Technology Process of methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate

There total 2 articles about methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

→ methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate (1042152-17-9)

Guidance literature:

Reference yield:

C20H36N2O2Si (1042151-93-8) + methyl 6-(chlorocarbonyl)picolinate (94111-79-2) → methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate (1042152-17-9)

Guidance literature:

C₂₀H₃₆N₂O₂Si; methyl 6-(chlorocarbonyl)picolinate; With triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 6h;

With p-toluenesulfonyl chloride; In 1,2-dichloro-ethane; at 80 ℃; for 16h; Inert atmosphere;

DOI:10.1021/jm800136b

Reference yield: 85.0%

methyl 6-(3-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate (1042152-17-9) → methyl 6-(3-(1-hydroxy-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate (1042152-19-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jm800136b

upstream raw materials:

C₂₀H₃₆N₂O₂Si

methyl 6-(chlorocarbonyl)picolinate

Downstream raw materials:

methyl 6-(3-(1-hydroxy-7-phenylheptyl)-1,2,4-oxadiazol-5-yl)-picolinate

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