1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone

Base Information

Chemical Name:1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone
CAS No.:60836-12-6
Molecular Formula:C₁₈H₂₆N₂O₂SSi₂
Molecular Weight:390.654
Hs Code.:

Synonyms:1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone

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Chemical Property of 1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone

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Technology Process of 1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone

There total 3 articles about 1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 60836-10-4
bis(trimethylsilylethynyl)ketone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 60836-12-6
1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone

Guidance literature:: With acetic acid; at 20 ℃;
DOI:10.1021/jo101125y

Reference yield:

: 13963-41-2
1,5-Bis(trimethylsilyl)-3-penta-1,4-diyn-3-ol

: 60836-12-6
1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / BaMnO₄ / CH₂Cl₂

2: 69 percent / acetic acid / Heating

With barium permanganate; In dichloromethane; acetic acid;
DOI:10.1021/jo00090a006

Reference yield:

: 54655-07-1
lithium trimethylsilylacetylenide

: 60836-12-6
1,5-Bis(trimethylsilyl)-1,4-pentadiyn-3-one (p-toluenesulfonyl)hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent

2: 94 percent / BaMnO₄ / CH₂Cl₂

3: 69 percent / acetic acid / Heating

With barium permanganate; In dichloromethane; acetic acid;
DOI:10.1021/jo00090a006