C₃₅H₄₆O₄Si

Base Information

Chemical Name:C₃₅H₄₆O₄Si
CAS No.:1373885-39-2
Molecular Formula:C₃₅H₄₆O₄Si
Molecular Weight:558.833
Hs Code.:

C<sub>35</sub>H<sub>46</sub>O<sub>4</sub>Si

Synonyms:C₃₅H₄₆O₄Si

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Chemical Property of C₃₅H₄₆O₄Si

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Technology Process of C₃₅H₄₆O₄Si

There total 10 articles about C₃₅H₄₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1373885-38-1
C₁₉H₂₈O₄

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1373885-39-2
C₃₅H₄₆O₄Si

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 5h;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: 81470-73-7
ethyl (4R,2E)-5-(benzyloxy)-4-methylpent-2-enoate

: 1373885-39-2
C₃₅H₄₆O₄Si

Guidance literature:: Multi-step reaction with 11 steps

1: AD-mix-α; methanesulfonamide; water / tert-butyl alcohol / 72 h / 0 °C

2: pyridinium p-toluenesulfonate / dichloromethane; acetone / 10 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

4: 1H-imidazole; iodine; triphenylphosphine / toluene / 20 h / 20 °C

5: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 4 h / -40 - 20 °C

6: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 72 h / 20 °C

7: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

8: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

9: methanol; potassium carbonate / 15 h / 20 °C

10: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

11: 1H-imidazole / dichloromethane / 5 h / 0 - 20 °C

With 1H-imidazole; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium periodate; copper(l) iodide; osmium(VIII) oxide; lithium aluminium tetrahydride; methanesulfonamide; AD-mix-α; water; iodine; pyridinium p-toluenesulfonate; zinc trifluoromethanesulfonate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 1: Sharpless asymmetric dihydroxylation / 8: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: 1373885-32-5
C₁₈H₂₆O₅

: 1373885-39-2
C₃₅H₄₆O₄Si

Guidance literature:: Multi-step reaction with 9 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2: 1H-imidazole; iodine; triphenylphosphine / toluene / 20 h / 20 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 4 h / -40 - 20 °C

4: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 72 h / 20 °C

5: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

6: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

7: methanol; potassium carbonate / 15 h / 20 °C

8: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

9: 1H-imidazole / dichloromethane / 5 h / 0 - 20 °C

With 1H-imidazole; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium periodate; copper(l) iodide; osmium(VIII) oxide; lithium aluminium tetrahydride; water; iodine; zinc trifluoromethanesulfonate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; 6: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090