N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide

Base Information

• Chemical Name: N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide
• CAS No.: 955938-09-7
• Molecular Formula: C₂₈H₄₂N₆O₂
• Molecular Weight: 494.68

Synonyms:N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide

Chemical Property of N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide

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Technology Process of N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide

There total 1 articles about N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4,10-bis[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester (1134189-81-3) → N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide (955938-09-7)

Guidance literature:

With hydrogen; palladium dihydroxide; In methanol; for 24h; under 2068.65 Torr;

DOI:10.1039/b710717j

Reference yield: 74.0%

N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide (955938-09-7) + 2-[6-(bromomethyl)pyridin-2-yl]-6-(tert-butyl)-10H-9-oxa-1-azaanthracen-10-one (1206963-37-2) → 7-[6-(6-tert-butyl-10-oxo-10H-9-oxa-1-aza-anthracen-2-yl)-pyridin-2-ylmethyl]-4,10-bis-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1-carboxylic acid tert-butyl ester

Guidance literature:

With potassium carbonate; In acetonitrile; for 16h; Inert atmosphere; Reflux;

Reference yield: 71.0%

2-(3-bromomethyl-1H-pyrazol-1-yl)-6-(tert-butyl)-10H-9-oxa-1-azaanthracen-10-one (955938-02-0) + N-((S)-1-phenyl-ethyl)-2-(7-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl)-acetamide (955938-09-7) → (S,S)-1-(7-tert-butyl-2-(pyrazoylmethyl)-1-azaxanthone)-4,10-(1-(1-phenyl)ethyl-carbamoylmethyl)-1,4,7,10-tetrazacyclododecane

Guidance literature:

With sodium hydrogencarbonate; In acetonitrile; at 60 ℃; for 18h;

DOI:10.1039/b709805g

upstream raw materials:

4,10-bis[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

Downstream raw materials:

4,10-bis-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1-carboxylic acid tert-butyl ester

4,10-bis-[((S)-1-phenyl-ethylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid di-tert-butyl ester

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