Lycophyll

Base Information

Chemical Name:Lycophyll
CAS No.:19891-75-9
Molecular Formula:C₄₀H₅₆O₂
Molecular Weight:568.883
Hs Code.:
UNII:6008SB6YF0
DSSTox Substance ID:DTXSID401318656
Nikkaji Number:J15.902F
Wikidata:Q27116463
Metabolomics Workbench ID:29022
Mol file:19891-75-9.mol

Synonyms:lycophyll

Suppliers and Price of Lycophyll

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Lycophyll

Chemical Property:

Melting Point:179°
Boiling Point:727.1±55.0 °C(Predicted)
PKA:14.52±0.10(Predicted)
Density:0.949±0.06 g/cm3(Predicted)
XLogP3:13.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:18
Exact Mass:568.42803102
Heavy Atom Count:42
Complexity:1100

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC=CC(=CC=CC(=CC=CC=C(C)C=CC=C(C)C=CC=C(C)CCC=C(C)CO)C)C)CCC=C(C)CO
Isomeric SMILES:C/C(=C\C=C\C(=C\C=C\C(=C\C=C\C=C(\C=C\C=C(\C=C\C=C(\CC/C=C(/CO)\C)/C)/C)/C)\C)\C)/CC/C=C(/CO)\C

Technology Process of Lycophyll

There total 9 articles about Lycophyll which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 40772-87-0
dimethyl Ψ,Ψ-carotene-16,16'-dioate

: 19891-75-9
16,16'-dihydroxylycopene

Guidance literature:: dimethyl Ψ,Ψ-carotene-16,16'-dioate; With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 1h;

With sodium hydroxide; water; In tetrahydrofuran; toluene; for 0.5h;

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 19891-75-9
16,16'-dihydroxylycopene

Guidance literature:: Multi-step reaction with 8 steps

1: selenium(IV) oxide / ethanol / Reflux; Inert atmosphere

2: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 20 °C / Inert atmosphere

3: potassium carbonate / water; methanol / 20 °C / Inert atmosphere

4: potassium carbonate / water; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

5: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6: ethyl acetate / 20 °C / Inert atmosphere

7: lithium methanolate / methanol; toluene / 24 h / Reflux; Inert atmosphere

8: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere

With selenium(IV) oxide; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; carbon tetrabromide; lithium methanolate; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 7: |Wittig Olefination;
DOI:10.1021/op050137f

Reference yield:

: 83852-61-3
(2E,6E)-8-acetoxy-2,6-dimethylocta-2,6-dienoic acid

: 19891-75-9
16,16'-dihydroxylycopene

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / water; methanol / 20 °C / Inert atmosphere

2: potassium carbonate / water; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4: ethyl acetate / 20 °C / Inert atmosphere

5: lithium methanolate / methanol; toluene / 24 h / Reflux; Inert atmosphere

6: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere

With carbon tetrabromide; lithium methanolate; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide; toluene; 5: |Wittig Olefination;
DOI:10.1021/op050137f