C₂₅H₂₂N₄O₈S₂

Base Information

Chemical Name:C₂₅H₂₂N₄O₈S₂
CAS No.:1093121-25-5
Molecular Formula:C₂₅H₂₂N₄O₈S₂
Molecular Weight:570.604
Hs Code.:

C<sub>25</sub>H<sub>22</sub>N<sub>4</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₂₅H₂₂N₄O₈S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₂N₄O₈S₂

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Technology Process of C₂₅H₂₂N₄O₈S₂

There total 10 articles about C₂₅H₂₂N₄O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1093121-47-1
C₂₆H₂₄N₄O₈S₂

: 1093121-25-5
C₂₅H₂₂N₄O₈S₂

Guidance literature:: C₂₆H₂₄N₄O₈S₂; With lithium hydroxide; water; In tetrahydrofuran; at 25 ℃;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield:

: 27828-71-3
5-hydroxynicotinic acid

: 1093121-25-5
C₂₅H₂₂N₄O₈S₂

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 18 h / 70 °C / Sealed tube; Heating / reflux

2: caesium carbonate / acetone / 18 h / 55 °C / Heating / reflux

3: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 25 °C

4: lithium hydroxide; water / tetrahydrofuran / 25 °C

With lithium hydroxide; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; N-ethyl-N,N-diisopropylamine; sulfuric acid; In tetrahydrofuran; dichloromethane; acetone;

Reference yield:

: 51933-78-9
5-bromo-2-(methylsulfanyl)pyridine

: 1093121-25-5
C₂₅H₂₂N₄O₈S₂

Guidance literature:: Multi-step reaction with 6 steps

1: Oxone / water; isopropyl alcohol / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 42 h / 80 - 120 °C

3: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 18 h / 25 °C

4: potassium carbonate / N,N-dimethyl-formamide / 120 h / 120 °C

5: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 25 °C

6: lithium hydroxide; water / tetrahydrofuran / 25 °C

With lithium hydroxide; Oxone; water; hydrogen; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;