Technology Process of 2,3-dimethyl-2-phenethyl-3-cyclopenten-1-one
There total 6 articles about 2,3-dimethyl-2-phenethyl-3-cyclopenten-1-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
nitromethane;
at 0 - 5 ℃;
for 0.5h;
DOI:10.1021/ja00398a022
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 70.5 percent / lithium diisopropylamide, HMPA / tetrahydrofuran / Ambient temperature
2: 5percent aq. sodium hydroxide / ethanol / 14 h / Heating
3: oxalyl chloride / benzene / 5 h / Ambient temperature
4: diethyl ether / Ambient temperature
5: 10 percent / boron trifluoride etherate / nitromethane / 0.5 h / 0 - 5 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; oxalyl dichloride; boron trifluoride diethyl etherate; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; nitromethane; ethanol; benzene;
DOI:10.1021/ja00398a022
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 70.5 percent / lithium diisopropylamide, HMPA / tetrahydrofuran / Ambient temperature
2: 5percent aq. sodium hydroxide / ethanol / 14 h / Heating
3: oxalyl chloride / benzene / 5 h / Ambient temperature
4: diethyl ether / Ambient temperature
5: 10 percent / boron trifluoride etherate / nitromethane / 0.5 h / 0 - 5 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; oxalyl dichloride; boron trifluoride diethyl etherate; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; nitromethane; ethanol; benzene;
DOI:10.1021/ja00398a022
