O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine

Base Information

Chemical Name:O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine
CAS No.:1392113-90-4
Molecular Formula:C₃₀H₆₁N₅O₈S
Molecular Weight:651.909
Hs Code.:

Synonyms:O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine

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Chemical Property of O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine

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Technology Process of O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine

There total 6 articles about O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1392113-72-2
O-3-deoxy-3-[[(1,1-dimethylethoxy)carbonyl]amino]-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,3,6-trideoxy-2,6-bis[[(1,1-dimethylethoxy)carbonyl]amino]-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-N¹,N³-bis[(1,1-dimethylethoxy)carbonyl]-D-streptamine

: 1392113-90-4
O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 0.05h;
DOI:10.1002/anie.201200761

Reference yield:

: 220612-64-6
((2R,3S,4S,5R,6S)-6-(((1S,2S,3R,4S,6R)-4,6-bis((tert-butoxycarbonyl)amino)-3-(((2R,3R,5S,6R)-3-((tert-butoxycarbonyl)methyl)-5-hydroxytetrahydro-2Hpyran-2-yl)oxy)-2-hydroxycyclohexyl)oxy)-4-((tert-butoxycarbonyl)amino)-3,5-dihydroxytetrahydro-2H-pyran-2-yl)methyl 2,4,6-triisopropylbenzenesulfonate

: 1392113-90-4
O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

2: trifluoroacetic acid / 0.05 h / 20 °C

With caesium carbonate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/anie.201200761

Reference yield:

: 112-55-0
1-dodecylthiol

: 1392113-90-4
O-3-amino-3-deoxy-6-S-dodecyl-6-thio-α-D-glucopyranosyl-(1→6)-O-[2,6-diamino-2,3,6-trideoxy-α-D-ribo-hexopyranosyl-(1→4)]-2-deoxy-D-streptamine

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / Heating

2: trifluoroacetic acid / neat (no solvent) / 20 °C

With caesium carbonate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1039/c2md20162c