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C39H54N4O7

Base Information
  • Chemical Name:C39H54N4O7
  • CAS No.:1388841-95-9
  • Molecular Formula:C39H54N4O7
  • Molecular Weight:690.88
  • Hs Code.:
C<sub>39</sub>H<sub>54</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:C39H54N4O7

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Chemical Property of C39H54N4O7
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Technology Process of C39H54N4O7

There total 6 articles about C39H54N4O7 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C20H28N2O5; C19H28N2O3; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h; Cooling;
With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h;
DOI:10.1039/c2cc32911e
Guidance literature:
Multi-step reaction with 5 steps
1.1: tetrahydrofuran / 5 h / 20 °C
2.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice
3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C
3.2: 6 h / 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice
5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C / Cooling
5.2: 4 h / 0 - 20 °C
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: Wittig reaction;
DOI:10.1039/c2cc32911e
Guidance literature:
Multi-step reaction with 3 steps
1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C
1.2: 6 h / 0 - 20 °C
2.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice
3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C / Cooling
3.2: 4 h / 0 - 20 °C
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc32911e
upstream raw materials:

C24H36N2O5

C22H32N2O5

C20H28N2O5

C19H28N2O3

Downstream raw materials:

C37H54N4O7

C54H76N6O9

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