(8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine

Base Information

Chemical Name:(8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine
CAS No.:1620137-44-1
Molecular Formula:C₂₈H₃₂N₄O₂
Molecular Weight:456.588
Hs Code.:

Synonyms:(8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine

Chemical Property:

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Technology Process of (8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine

There total 6 articles about (8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₃H₄₂N₄O₄

: 1620137-44-1
(8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine

Guidance literature:: With piperidine; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2014.05.003

Reference yield:

: (8S,9S)-9-azide(9-deoxy)-epi-cinchonidine

: 1620137-44-1
(8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine / tetrahydrofuran / 4 h / 48 - 52 °C

2: tetrahydrofuran / 1 h / 20 °C

3: piperidine / N,N-dimethyl-formamide

With piperidine; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; 1: |Staudinger Azide Reduction;
DOI:10.1016/j.tetasy.2014.05.003

Reference yield:

: 560119-42-8
(8S,9R)-9-O-mesylcinchonidine

: 1620137-44-1
(8S,9S)-9-L-tyrosinylamide(9-deoxy)-epi-cinchonidine

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / N,N-dimethyl-formamide / 24 h / 80 °C

2: triphenylphosphine / tetrahydrofuran / 4 h / 48 - 52 °C

3: tetrahydrofuran / 1 h / 20 °C

4: piperidine / N,N-dimethyl-formamide

With piperidine; sodium azide; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: |Staudinger Azide Reduction;
DOI:10.1016/j.tetasy.2014.05.003