6-AMINO-1-(2-CHLOROPHENYL)-2-THIOXO-2,3-DIHYDRO-4(1H)-PYRIMIDINONE

Base Information

• Chemical Name: 6-AMINO-1-(2-CHLOROPHENYL)-2-THIOXO-2,3-DIHYDRO-4(1H)-PYRIMIDINONE
• CAS No.: 180028-92-6
• Molecular Formula: C₁₀H₈ClN₃OS
• Molecular Weight: 253.712
• Mol file: 180028-92-6.mol

Synonyms:6-amino-1-(2-chlorophenyl)-2,3-dihydro-2-thioxopyrimidine-4-one

Chemical Property of 6-AMINO-1-(2-CHLOROPHENYL)-2-THIOXO-2,3-DIHYDRO-4(1H)-PYRIMIDINONE

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 6-AMINO-1-(2-CHLOROPHENYL)-2-THIOXO-2,3-DIHYDRO-4(1H)-PYRIMIDINONE

There total 1 articles about 6-AMINO-1-(2-CHLOROPHENYL)-2-THIOXO-2,3-DIHYDRO-4(1H)-PYRIMIDINONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

ethyl 2-cyanoacetate (105-56-6) + o-chlorophenylthiourea (5344-82-1) → 6-amino-1-(2-chlorophenyl)-2,3-dihydro-2-thioxopyrimidine-4-one (180028-92-6)

Guidance literature:

With sodium ethanolate; In ethanol; for 4h; Heating;

DOI:10.1080/10426500008043681

Reference yield: 92.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 6-amino-1-(2-chlorophenyl)-2,3-dihydro-2-thioxopyrimidine-4-one (180028-92-6) + Cyclopentamine (1003-03-8) → 1-(2-chlorophenyl)-6-cyclopentyl-2-thioxo-2,3,5,6,7,8-hexahydropyrimido[4,5-d]pyrimidin-4(1H)-one (879771-60-5)

Guidance literature:

In water; N,N-dimethyl-formamide; at 20 - 25 ℃; for 8h;

DOI:10.1007/s11172-008-0199-0

Reference yield: 84.0%

6-amino-1-(2-chlorophenyl)-2,3-dihydro-2-thioxopyrimidine-4-one (180028-92-6) + 1,1'-di-pyridin-3-yl-3,3'-p-phenylene-bis-propenone (98822-34-5) → C42H24Cl2N8O2S2

Guidance literature:

With piperidine; In ethanol; for 3h; Heating;

DOI:10.1080/10426500008043681

upstream raw materials:

ethyl 2-cyanoacetate

o-chlorophenylthiourea

Downstream raw materials:

6-amino-1-(2-chlorophenyl)-5-nitroso-2-thioxo-2,3-dihydropyrimidin-4(1H)-one

1-(2-chlorophenyl)-6-phenethyl-2-thioxo-2,3,5,6,7,8-hexahydropyrimido[4,5-d]pyrimidin-4(1H)-one

1-(2-chlorophenyl)-6-cyclopentyl-2-thioxo-2,3,5,6,7,8-hexahydropyrimido[4,5-d]pyrimidin-4(1H)-one

5,6-diamino-1-(2-chlorophenyl)-2-thioxo-2,3-dihydropyrimidin-4(1H)-one

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