p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside
CAS No.:1357000-53-3
Molecular Formula:C₄₀H₅₇NO₁₇S
Molecular Weight:855.955
Hs Code.:

Synonyms:p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

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Chemical Property of p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

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Technology Process of p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

There total 5 articles about p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1357000-52-2
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

: 108-24-7
acetic anhydride

: 1357000-53-3
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

Guidance literature:: With pyridine; dmap; at 0 - 20 ℃; for 2h;
DOI:10.3987/COM-11-12332

Reference yield:

: 1242660-03-2
3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-2)-D-glucosaminyl-3-O-benzyl-(4,6)-benzylidene-β-D-mannopyranosyl p-octyloxyphenyl sulfoxide

: 1357000-53-3
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: triphenylphosphine / tetrachloromethane; acetonitrile / 2 h / Reflux

2: hydrazine hydrate / ethanol; water; toluene / 5 h / Reflux

3: pyridine / 5 h

4: acetic acid / tetrahydrofuran; water / 5 h / 55 °C

5: chloro-trimethyl-silane; lithium iodide / chloroform / 6 h / 0 - 20 °C

6: pyridine; dmap / 2 h / 0 - 20 °C

With pyridine; dmap; chloro-trimethyl-silane; hydrazine hydrate; acetic acid; triphenylphosphine; lithium iodide; In tetrahydrofuran; tetrachloromethane; ethanol; chloroform; water; toluene; acetonitrile;
DOI:10.3987/COM-11-12332

Reference yield:

: C₄₆H₅₉NO₁₃S

: 1357000-53-3
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 5 h

2: acetic acid / tetrahydrofuran; water / 5 h / 55 °C

3: chloro-trimethyl-silane; lithium iodide / chloroform / 6 h / 0 - 20 °C

4: pyridine; dmap / 2 h / 0 - 20 °C

With pyridine; dmap; chloro-trimethyl-silane; acetic acid; lithium iodide; In tetrahydrofuran; chloroform; water;
DOI:10.3987/COM-11-12332