ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate

Base Information

• Chemical Name: ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate
• CAS No.: 1155808-03-9
• Molecular Formula: C₂₂H₂₄BrF₃O₃
• Molecular Weight: 473.33

Synonyms:ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate

Chemical Property of ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate

Chemical Property:

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Technology Process of ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate

There total 1 articles about ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Isobutyl bromide (78-77-3) + ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)acetate (1155808-01-7) → ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate (1155808-03-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.75h;

Reference yield:

ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate (1155808-03-9) + benzo[c][1,2,5]oxadiazole-5-boronic acid (426268-09-9) → ethyl 2-(3-benzo[c][1,2,5]oxadiazol-5-yl)-5-(4-(trifluoromethyl)benzyloxy)phenyl-4-methylpentanoate (1155808-05-1)

Guidance literature:

With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 80 ℃; for 8h;

Reference yield:

benzo[c][1,2,5]thiadiazol-5-ylboronic acid (191341-04-5) + ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)-4-methylpentanoate (1155808-03-9) → ethyl 2-(3-benzo[c][1,2,5]thiadiazol-5-yl)-5-(4-(trifluoromethyl)benzyloxy)phenyl-4-methyl pentanoate (1155808-07-3)

Guidance literature:

With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 80 ℃; for 8h;

upstream raw materials:

Isobutyl bromide

ethyl 2-(3-bromo-5-(4-(trifluoromethyl)benzyloxy)phenyl)acetate

Downstream raw materials:

ethyl 2-(3-benzo[c][1,2,5]oxadiazol-5-yl)-5-(4-(trifluoromethyl)benzyloxy)phenyl-4-methylpentanoate

ethyl 2-(3-benzo[c][1,2,5]thiadiazol-5-yl)-5-(4-(trifluoromethyl)benzyloxy)phenyl-4-methyl pentanoate

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