benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:1071226-05-5
Molecular Formula:C₁₀₃H₁₀₂N₂O₂₂
Molecular Weight:1719.94
Hs Code.:

benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Synonyms:benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 2 articles about benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1071226-12-4
benzyl 2,4-di-O-benzyl-3,6-di-O-levulinoyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 1071226-05-5
benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With hydrazinium monoacetate; In methanol; dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1002/chem.200800757

Reference yield: 74.0%

: benzyl O-2,4-di-O-benzyl-3,6-di-O-(para-methoxybenzyl)-β-D-mannopyranosyl-(1→4)-O-3,6-di-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-gluopyranosyl-(1→4)-O-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1→6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-gluopyranoside

: 1071226-05-5
benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 3h; pH=7; Inert atmosphere;
DOI:10.1002/ejoc.202000313

Reference yield: 95.0%

: 1071226-05-5
benzyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->6))-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 74808-09-6,90357-89-4,90358-01-3,103368-01-0,103368-04-3,103368-06-5,104048-30-8,104048-33-1,114743-70-3,132201-75-3,132748-02-8,83441-60-5
2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl trichloroacetimidate

: benzyl O-2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1→3)-O-[2-Obenzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1→6)]-O-2,4-di-O-benzyl-β-Dmannopyranosyl-(1→4)-O-3,6-di-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-Dgluopyranosyl-(1→4)-O-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1→6)]-3-Obenzyl-2-deoxy-2-phthalimido-β-D-gluopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.202000313