1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride

Base Information

• Chemical Name: 1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride
• CAS No.: 107037-63-8
• Molecular Formula: C₁₄H₂₀N₃O₃S*Cl
• Molecular Weight: 345.85

Synonyms:1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride

Chemical Property of 1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride

Chemical Property:

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Technology Process of 1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride

There total 3 articles about 1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

1-[2-(4-Ethanesulfonylamino-phenyl)-2-oxo-ethyl]-3-methyl-3H-imidazol-1-ium; chloride (107037-53-6) → 1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride (107037-63-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In water; for 5h; under 2585.7 Torr; Ambient temperature;

DOI:10.1021/jm00387a020

Reference yield:

N-phenyl-S-ethylsulfonamide (2225-19-6) → 1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride (107037-63-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / aluminum chloride / CH₂Cl₂ / 7 h / -10 - 20 °C

2: 76 percent / acetonitrile / 17 h / Heating

3: 66 percent / H₂ / 10percent Pd/C / H₂O / 5 h / 2585.7 Torr / Ambient temperature

With aluminium trichloride; hydrogen; palladium on activated charcoal; In dichloromethane; water; acetonitrile;

DOI:10.1021/jm00387a020

Reference yield:

Ethanesulfonic acid [4-(2-chloro-acetyl)-phenyl]-amide (107037-69-4) → 1-[2-(4-Ethanesulfonylamino-phenyl)-2-hydroxy-ethyl]-3-methyl-3H-imidazol-1-ium; chloride (107037-63-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / acetonitrile / 17 h / Heating

2: 66 percent / H₂ / 10percent Pd/C / H₂O / 5 h / 2585.7 Torr / Ambient temperature

With hydrogen; palladium on activated charcoal; In water; acetonitrile;

DOI:10.1021/jm00387a020

upstream raw materials:

1-[2-(4-Ethanesulfonylamino-phenyl)-2-oxo-ethyl]-3-methyl-3H-imidazol-1-ium; chloride

N-phenyl-S-ethylsulfonamide

Ethanesulfonic acid [4-(2-chloro-acetyl)-phenyl]-amide

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