2-cyclohexylethynylbenzyl alcohol

Base Information

Chemical Name:2-cyclohexylethynylbenzyl alcohol
CAS No.:1319735-03-9
Molecular Formula:C₁₅H₁₈O
Molecular Weight:214.307
Hs Code.:

Synonyms:2-cyclohexylethynylbenzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-cyclohexylethynylbenzyl alcohol

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Technology Process of 2-cyclohexylethynylbenzyl alcohol

There total 1 articles about 2-cyclohexylethynylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 931-48-6
2-cyclohexylacetylene

: 5159-41-1
2-iodobenzyl alcohol

: 1319735-03-9
2-cyclohexylethynylbenzyl alcohol

Guidance literature:: With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In toluene; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1039/c1cc13094c

Reference yield: 45.0%

: 1319735-03-9
2-cyclohexylethynylbenzyl alcohol

: 1319735-07-3
2-cyclohexylethynylbenzyl bromide

Guidance literature:: With pyridine; phosphorus tribromide; In chloroform; at 0 - 20 ℃;
DOI:10.1039/c1cc13094c

Reference yield:

: 1319735-03-9
2-cyclohexylethynylbenzyl alcohol

: 1319735-17-5
1-(2-cyclohexylethynylbenzyl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; phosphorus tribromide / chloroform / 0 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

With pyridine; phosphorus tribromide; sodium hydride; In chloroform; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c1cc13094c