2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Base Information

• Chemical Name: 2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside
• CAS No.: 357674-81-8
• Molecular Formula: C₄₃H₅₇F₃N₂O₂₅
• Molecular Weight: 1058.92
• Mol file: 357674-81-8.mol

Synonyms:2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Chemical Property of 2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

There total 1 articles about 2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(p-trifluoroacetamidophenyl)ethyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->3)-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside → 2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside (357674-81-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; acetic acid; at 20 ℃; for 20h; under 258.574 Torr;

DOI:10.1081/CAR-100102540

Reference yield: 62.0%

2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside (357674-81-8) → 2-(p-aminophenyl)ethyl (5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside + 2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Guidance literature:

With methanol; sodium;

DOI:10.1081/CAR-100102540

Reference yield:

2-(p-trifluoroacetamidophenyl)ethyl (5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(2-O-acetyl-β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside (357674-81-8) → 2-(p-aminophenyl)ethyl (5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid)-(2->3)-(β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Guidance literature:

Multi-step reaction with 2 steps

1: 62 percent / Na; MeOH

2: 76 percent / NH₄OH / 20 °C

With methanol; ammonium hydroxide; sodium;

DOI:10.1081/CAR-100102540