N¹,N²-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester

Base Information

• Chemical Name: N¹,N²-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester
• CAS No.: 190016-72-9
• Molecular Formula: C₃₀H₂₈N₂S₂
• Molecular Weight: 480.698

Synonyms:N¹,N²-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester

Chemical Property of N¹,N²-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester

Chemical Property:

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Technology Process of N¹,N²-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester

There total 1 articles about N¹,N²-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

di(p-tolyl) disulfide (103-19-5) + 4-methylphenyl isocyanide (7175-47-5) → (CH3C6H4S)2CN(C6H4CH3) (190016-70-7) + N1,N2-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester (190016-72-9) + N1,N3-Di-p-tolyl-2-p-tolylimino-dithiomalonodiimidic acid di-p-tolyl ester (190016-71-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 80 ℃; for 14h;

DOI:10.1021/ja970518b

Reference yield: 64.0%

tetrakis(triphenylphosphine)platinum (14221-02-4) + N1,N2-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester (190016-72-9) → Pt[(CNC6H4CH3)2(SC6H4CH3)](SC6H4CH3)[P(C6H5)3]2

Guidance literature:

In benzene-d6; (Ar); NMR tube (12 h, 50°C); recrystn. (benzene/hexane);

DOI:10.1021/ja970518b

Reference yield: 27.0%

4-methylphenyl isocyanide (7175-47-5) + N1,N2-Di-p-tolyl-dithiooxalodiimidic acid di-p-tolyl ester (190016-72-9) → N1,N3-Di-p-tolyl-2-p-tolylimino-dithiomalonodiimidic acid di-p-tolyl ester (190016-71-8) + N1,N4-Di-p-tolyl-2,3-bis-[(Z)-p-tolylimino]-dithiosuccinodiimidic acid di-p-tolyl ester

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 80 ℃; for 24h;

DOI:10.1021/ja970518b

upstream raw materials:

di(p-tolyl) disulfide

4-methylphenyl isocyanide

Downstream raw materials:

N¹,N³-Di-p-tolyl-2-p-tolylimino-dithiomalonodiimidic acid di-p-tolyl ester

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