S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate

Base Information

Chemical Name:S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate
CAS No.:1417621-82-9
Molecular Formula:C₂₃H₂₄N₂O₅S₂
Molecular Weight:472.586
Hs Code.:

Synonyms:S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate

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Technology Process of S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate

There total 2 articles about S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 19194-55-9
O-ethyl S-phthalimidomethyl dithiocarbonate

: 5041-33-8
N-(Benzyloxycarbonyl)allylamine

: 1417621-82-9
S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate

Guidance literature:: With dilauryl peroxide; In 1,2-dichloro-ethane; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.11.074

Reference yield:

: 17564-64-6
N-(chloromethyl)phthalimide

: 1417621-82-9
S-1-benzoxycarbonylamino-4-phthalimidobutan-2-yl O-ethyl dithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 10 h / 20 °C / Cooling with ice

2: dilauryl peroxide / 1,2-dichloro-ethane / Inert atmosphere; Reflux

With dilauryl peroxide; In 1,2-dichloro-ethane; acetone;
DOI:10.1016/j.tet.2012.11.074