methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate

Base Information

Chemical Name:methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate
CAS No.:907587-42-2
Molecular Formula:C₂₁H₁₆Cl₂N₂O₅S
Molecular Weight:479.34
Hs Code.:

Synonyms:methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate

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Chemical Property of methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate

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Technology Process of methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate

There total 4 articles about methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 136402-32-9
5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoic acid

: 619-45-4
4-methoxycarbonyl aniline

: 907587-42-2
methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 96h;
DOI:10.1016/j.bmc.2006.04.038

Reference yield:

: 907587-41-1
methyl 5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoate

: 907587-42-2
methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaOH / methanol; 1,2-dimethoxy-ethane; tetrahydrofuran / 5 h / 50 °C

2: 48 percent / EDC*HCl; 4-dimethylaminopyridine / CH₂Cl₂ / 96 h / 20 °C

With dmap; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/j.bmc.2006.04.038

Reference yield:

: 5202-89-1
4-chlorobenzenesulfonyl chloride

: 907587-42-2
methyl 4-[(5-chloro-2-{[(4-chlorophenyl)sulfonyl]amino}benzoyl)amino]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / pyridine / CH₂Cl₂ / 3 h / 20 °C

2: 98 percent / NaOH / methanol; 1,2-dimethoxy-ethane; tetrahydrofuran / 5 h / 50 °C

3: 48 percent / EDC*HCl; 4-dimethylaminopyridine / CH₂Cl₂ / 96 h / 20 °C

With pyridine; dmap; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/j.bmc.2006.04.038