C₃₄H₅₀N₆O₁₀

Base Information

Chemical Name:C₃₄H₅₀N₆O₁₀
CAS No.:1579275-68-5
Molecular Formula:C₃₄H₅₀N₆O₁₀
Molecular Weight:702.805
Hs Code.:

C<sub>34</sub>H<sub>50</sub>N<sub>6</sub>O<sub>10</sub>

Synonyms:C₃₄H₅₀N₆O₁₀

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Chemical Property of C₃₄H₅₀N₆O₁₀

Chemical Property:

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Technology Process of C₃₄H₅₀N₆O₁₀

There total 10 articles about C₃₄H₅₀N₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1579275-65-2
C₃₇H₅₄N₆O₁₀

: 1579275-68-5
C₃₄H₅₀N₆O₁₀

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo500039d

Reference yield:

: 1515605-52-3
C₁₄H₂₉N₃O₂Si

: 1579275-68-5
C₃₄H₅₀N₆O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: triethylphosphine / tetrahydrofuran; toluene / 30 h / 20 °C / Inert atmosphere

2: toluene / 48 h / 70 °C / Inert atmosphere

3: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere

4: triethylamine; dmap / acetonitrile / Inert atmosphere

5: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / 2,2,2-trifluoroethanol / 1 h / -78 °C / Inert atmosphere

6: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With morpholine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine tris(hydrogen fluoride); triethylamine; triethylphosphine; In tetrahydrofuran; 2,2,2-trifluoroethanol; toluene; acetonitrile; 1: |Staudinger Azide Reduction / 2: |Ugi Condensation;
DOI:10.1021/jo500039d

Reference yield:

: C₁₇H₂₄N₂O₆

: 1579275-68-5
C₃₄H₅₀N₆O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2: toluene / 48 h / 70 °C / Inert atmosphere

3: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere

4: triethylamine; dmap / acetonitrile / Inert atmosphere

5: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / 2,2,2-trifluoroethanol / 1 h / -78 °C / Inert atmosphere

6: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With morpholine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydrogencarbonate; triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; 2,2,2-trifluoroethanol; N,N-dimethyl-formamide; toluene; acetonitrile; 2: |Ugi Condensation;
DOI:10.1021/jo500039d