(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide

Base Information

• Chemical Name: (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide
• CAS No.: 960060-67-7
• Molecular Formula: C₂₁H₂₂F₃NO₃
• Molecular Weight: 393.406

Synonyms:(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide

Chemical Property of (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide

Chemical Property:

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Technology Process of (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide

There total 2 articles about (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C21H22F3NO3 (960060-53-1) → (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide (960060-67-7)

Guidance literature:

With di-μ-chlorobis[η⁵-(S)-(S_p)-2-(2'-(4'-methylethyl)oxazolinyl)cyclopentadienyl, (1-C,3'-N)(η⁵-pentaphenylcyclopentadiene)ferrocene]dipalladium; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; silver nitrate; In dichloromethane; at 50 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.200900712

Reference yield: 84.0%

(Z)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-5-benzyloxypent-2-enyl ester → (R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(benzyloxymethyl-1-methyl-1-allyl)acetamide (960060-67-7)

Guidance literature:

With silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; ferrocenyl 1-Ts-2,3-Ph₂-imidazoline palladacycle catalyst; In dichloromethane; at 50 ℃; for 60h;

DOI:10.1002/anie.200702086

upstream raw materials:

C₂₁H₂₂F₃NO₃

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