2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1181210-11-6
Molecular Formula:C₂₁H₃₅BO₇
Molecular Weight:410.316
Hs Code.:

Synonyms:2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 110429-45-3,92450-98-1
1-{2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxy}-2-methoxy-ethane

: 269409-70-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1181210-11-6
2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 65h;

Reference yield: 94.0%

: C₅₀H₆₄F₃N₅O₁₃SSi₂

: 1181210-11-6
2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: (R)-2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-8-((5-(((R)-2-(4-aminophenyl)-7-methoxy-5,11-dioxo-10-((2-(trimethylsilyl)ethoxy)methyl)-5,10,11,11a-tetrahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-8-yl)oxy)pentyl)oxy)-7-methoxy-10-((2-(trimethylsilyl)ethoxy)methyl)-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11(10H,11aH)-dione

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; toluene; at 20 ℃; for 3h;

Reference yield: 89.2%

: 1181210-11-6
2-(4-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: C₄₉H₄₇BrN₈O₃

: C₆₄H₇₀N₈O₈

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 90 ℃; for 24h; Schlenk technique; Sealed tube;
DOI:10.1039/c6tc02557a