(Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Base Information

• Chemical Name: (Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal
• CAS No.: 1256752-71-2
• Molecular Formula: C₁₈H₂₄O₃Si
• Molecular Weight: 316.472

Synonyms:(Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Chemical Property of (Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of (Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal

There total 1 articles about (Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C21H30O2S2Si → (Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal (1256752-71-2)

Guidance literature:

With water; calcium carbonate; methyl iodide; In acetonitrile; at 60 ℃; Inert atmosphere;

DOI:10.1021/ol102278c

Reference yield: 76.0%

(Z)-4-(4-(dimethylphenylsilyl)-2-oxodihydrofuran-3(2H)-ylidene)-2,2-dimethylbutanal (1256752-71-2) → rac-(3S,4R)-4-(dimethyl(phenyl)silyl)-3-((1S,2S)-2-hydroxy-3,3-dimethylcyclobutyl)dihydrofuran-2(3H)-one + rac-(3S,4R)-4-(dimethyl(phenyl)silyl)-3-((1R,2R)-2-hydroxy-3,3-dimethylcyclobutyl)dihydrofuran-2(3H)-one

Guidance literature:

With methanol; samarium diiodide; In tetrahydrofuran; at 0 ℃; for 0.166667h; optical yield given as %de; diastereoselective reaction;

DOI:10.1021/ol102278c

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