C₃₂H₃₇N₃O₅SSi

Base Information

Chemical Name:C₃₂H₃₇N₃O₅SSi
CAS No.:1181080-53-4
Molecular Formula:C₃₂H₃₇N₃O₅SSi
Molecular Weight:603.814
Hs Code.:

C<sub>32</sub>H<sub>37</sub>N<sub>3</sub>O<sub>5</sub>SSi

Synonyms:C₃₂H₃₇N₃O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₃₇N₃O₅SSi

Chemical Property:

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Technology Process of C₃₂H₃₇N₃O₅SSi

There total 17 articles about C₃₂H₃₇N₃O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1181080-52-3
C₃₂H₃₉N₃O₅SSi

: 1181080-53-4
C₃₂H₃₇N₃O₅SSi

Guidance literature:: With Montmorillonite K₁₀; bis-[(trifluoroacetoxy)iodo]benzene; In 2,2,2-trifluoroethanol; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol901471r

Reference yield:

: 55149-84-3
2-nitroveratraldehyde

: 1181080-53-4
C₃₂H₃₇N₃O₅SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 1.25 h / -2 °C

2.1: palladium on carbon; formic acid; ammonium formate / methanol / 1 h

3.1: 2 h / 0 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / Reflux

5.1: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 9 h

6.1: potassium tert-butylate / tetrahydrofuran / 6 h / 0 °C

7.1: 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; bis-[(trifluoroacetoxy)iodo]benzene / water / 1 h / 0 °C

8.1: hydrogenchloride / methanol / 0.5 h / 20 °C / Inert atmosphere

8.2: 16 h / 20 °C / Inert atmosphere

9.1: bis-[(trifluoroacetoxy)iodo]benzene / 2,2,2-trifluoroethanol / 0.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; formic acid; 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; diphenyl phosphoryl azide; palladium on carbon; potassium tert-butylate; ammonium formate; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; potassium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; 2,2,2-trifluoroethanol; water; N,N-dimethyl-formamide; toluene; 5.1: Mitsunobu reaction;
DOI:10.1039/c1ob05058c

Reference yield:

: 1181080-76-1
C₂₈H₂₇NO₂

: 1181080-53-4
C₃₂H₃₇N₃O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2.5 h / 0 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.1: hydrogenchloride / methanol / 0.5 h / 20 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: bis-[(trifluoroacetoxy)iodo]benzene / 2,2,2-trifluoroethanol / 0.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; methanol; dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1039/c1ob05058c