8,11-dioxa-5,14-dithia-2⁽³⁾,2⁽³⁾,2⁽⁴⁾,2⁽⁴⁾,2⁽⁵⁾,2⁽⁵⁾-hexafluoro-1⁽³⁾,1⁽⁵⁾,3⁽³⁾,3⁽⁵⁾-tetramethyl-2(1,2)-cyclopentena-1,3(2,4)dithiophenacyclopentadecaphane

Base Information

• Chemical Name: 8,11-dioxa-5,14-dithia-2⁽³⁾,2⁽³⁾,2⁽⁴⁾,2⁽⁴⁾,2⁽⁵⁾,2⁽⁵⁾-hexafluoro-1⁽³⁾,1⁽⁵⁾,3⁽³⁾,3⁽⁵⁾-tetramethyl-2(1,2)-cyclopentena-1,3(2,4)dithiophenacyclopentadecaphane
• CAS No.: 1134600-73-9
• Molecular Formula: C₂₅H₂₈F₆O₂S₄
• Molecular Weight: 602.751

Synonyms:8,11-dioxa-5,14-dithia-2⁽³⁾,2⁽³⁾,2⁽⁴⁾,2⁽⁴⁾,2⁽⁵⁾,2⁽⁵⁾-hexafluoro-1⁽³⁾,1⁽⁵⁾,3⁽³⁾,3⁽⁵⁾-tetramethyl-2(1,2)-cyclopentena-1,3(2,4)dithiophenacyclopentadecaphane

Chemical Property of 8,11-dioxa-5,14-dithia-2⁽³⁾,2⁽³⁾,2⁽⁴⁾,2⁽⁴⁾,2⁽⁵⁾,2⁽⁵⁾-hexafluoro-1⁽³⁾,1⁽⁵⁾,3⁽³⁾,3⁽⁵⁾-tetramethyl-2(1,2)-cyclopentena-1,3(2,4)dithiophenacyclopentadecaphane

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Technology Process of 8,11-dioxa-5,14-dithia-2⁽³⁾,2⁽³⁾,2⁽⁴⁾,2⁽⁴⁾,2⁽⁵⁾,2⁽⁵⁾-hexafluoro-1⁽³⁾,1⁽⁵⁾,3⁽³⁾,3⁽⁵⁾-tetramethyl-2(1,2)-cyclopentena-1,3(2,4)dithiophenacyclopentadecaphane

There total 1 articles about 8,11-dioxa-5,14-dithia-2⁽³⁾,2⁽³⁾,2⁽⁴⁾,2⁽⁴⁾,2⁽⁵⁾,2⁽⁵⁾-hexafluoro-1⁽³⁾,1⁽⁵⁾,3⁽³⁾,3⁽⁵⁾-tetramethyl-2(1,2)-cyclopentena-1,3(2,4)dithiophenacyclopentadecaphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

{5-[3,3,4,4,5,5-hexafluoro-2-(4-mercaptomethyl-3,5-dimethyl-thiophen-2-yl)-cyclopent-1-enyl]-2,4-dimethyl-thiophen-3-yl}-methanethiol (756873-38-8) + triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 8,11-dioxa-5,14-dithia-2(3),2(3),2(4),2(4),2(5),2(5)-hexafluoro-1(3),1(5),3(3),3(5)-tetramethyl-2(1,2)-cyclopentena-1,3(2,4)dithiophenacyclopentadecaphane (1134600-73-9)

Guidance literature:

With potassium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; ethanol; Reflux;

DOI:10.1039/b823492b

upstream raw materials:

{5-[3,3,4,4,5,5-hexafluoro-2-(4-mercaptomethyl-3,5-dimethyl-thiophen-2-yl)-cyclopent-1-enyl]-2,4-dimethyl-thiophen-3-yl}-methanethiol

triethylene glycol di-(p-toluenesulfonate)

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