1-phenethylcyclohexan-1-amine

Base Information

Chemical Name:1-phenethylcyclohexan-1-amine
CAS No.:764588-50-3
Molecular Formula:C₁₄H₂₁N
Molecular Weight:203.327
Hs Code.:

Synonyms:1-phenethylcyclohexan-1-amine

Suppliers and Price of 1-phenethylcyclohexan-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-phenethylcyclohexan-1-amine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of 1-phenethylcyclohexan-1-amine

There total 5 articles about 1-phenethylcyclohexan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 108-91-8,157973-60-9
cyclohexylamine

: 764588-50-3
1-phenethylcyclohexan-1-amine

Guidance literature:: With 3,5-difluoro-2,4,6-tris(N-phenylanilino)benzonitrile; tetrabutylammoniun azide; In N,N-dimethyl-formamide; at 25 - 26 ℃; for 20h; Reagent/catalyst; Catalytic behavior; Quantum yield; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1021/jacs.1c07401

Reference yield: 62.0%

: 591-50-4
iodobenzene

: 2626-60-0
1-ethylcyclohexan-1-amine

: 764588-50-3
1-phenethylcyclohexan-1-amine

Guidance literature:: With carbon dioxide; water; palladium diacetate; silver trifluoroacetate; acetic acid; at 110 ℃; for 13h; Sealed tube;
DOI:10.1021/jacs.8b05061

Reference yield:

: 1940-18-7
1-ethylcyclohexanol

: 764588-50-3
1-phenethylcyclohexan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; trifluoroacetic acid / chloroform / -5 - 0 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

3: palladium diacetate; silver trifluoroacetate; acetic acid; water; carbon dioxide / 13 h / 110 °C / Sealed tube

With lithium aluminium tetrahydride; sodium azide; carbon dioxide; water; palladium diacetate; silver trifluoroacetate; acetic acid; trifluoroacetic acid; In tetrahydrofuran; chloroform;
DOI:10.1021/jacs.8b05061