3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

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Chemical Name:3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate
CAS No.:1373878-00-2
Molecular Formula:C₅₉H₇₂ClNO₉
Molecular Weight:974.675
Hs Code.:

Synonyms:3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

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Chemical Property of 3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

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Technology Process of 3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

There total 9 articles about 3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1373878-51-3
3-amino-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

: 868620-29-5
4-(2`hydroxy-4`-dodecylhydroxybenzoylhydroxy)benzaldehyde

: 1373878-00-2
3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

Guidance literature:: With acetic acid; In ethanol; at 20 ℃; for 24h;
DOI:10.3762/bjoc.8.15

Reference yield:

: 1373878-40-0
4-formylphenyl 3-chloro-4-n-dodecyloxybenzoate

: 1373878-00-2
3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: dihydrogen peroxide; acetic acid / water / 22 h / 40 - 75 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C

3: 10 wt % palladium on activated carbon; hydrogen / ethyl acetate

4: acetic acid / ethanol / 24 h / 20 °C

With dmap; 10 wt % palladium on activated carbon; hydrogen; dihydrogen peroxide; acetic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water; ethyl acetate;
DOI:10.3762/bjoc.8.15

Reference yield:

: 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoic acid

: 1373878-00-2
3-[4-(4-n-dodecyloxybenzoyloxy)-2-hydroxybenzylideneamino]-2-methylphenyl 4-(3-chloro-4-n-dodecyloxybenzoyloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C

2: 10 wt % palladium on activated carbon; hydrogen / ethyl acetate

3: acetic acid / ethanol / 24 h / 20 °C

With dmap; 10 wt % palladium on activated carbon; hydrogen; acetic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; ethyl acetate;
DOI:10.3762/bjoc.8.15